Details, Fiction and tga66
Details, Fiction and tga66
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以下因為這次忘記拍照，先用一些示意圖，等之後修理其他支的機會，再來補照片
However, the steady multilayer carbonaceous chars (Determine 5) generated within the response concerning HCNP along with the decomposition merchandise of PA66 can insulate the fundamental substrate in the warmth source and decelerate the two the warmth and mass transfer [twenty five]. Hence, it could be summarized that HCNP can efficiently Increase the flame retardancy of PA66 following the gas-period flame retardant system.
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Recently, polyphosphazene derivatives happen to be verified to be essentially the most prospective flame retardants owing for their designability and char development. By way of example, novel cross-linked polyphosphazene microspheres were being synthesized with 4,four′-dihydroxy biphenyl and tannic acid as co-monomers and decorated with layered double hydroxide to Enhance the flame retardancy from the epoxy resin. The results unveiled which the EP containing four.0 wt% microspheres exhibited the highest LOI of 29.
These properties can improve the fire resistance and char formation of polyamide in the combustion procedure owing for their certain flame retardant mechanism [nine]. Nevertheless, the minimal degradation temperature in the elementary material in phosphorus-type flame retardants restrictions their application within the processing of polyamide [10].
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PA66 pellets and HCNP powder were being dried for four h at a hundred °C before extrusion. The FR-PA66 was prepared by twin-screw extrusion response in the variety of 260–270 °C. The take a look at samples ended up produced utilizing a TTI-95G injection molding equipment beneath 265 °C by using a a hundred and eighty r/min rotation velocity. Figure 6 reveals the microtopography of pure PA66, HCNP, and FR-PA66. It could be noticed from Determine 6c that the HCNP microspheres have been dispersed much more uniformly without the need of noticeable stage interfaces, along with the peeling phenomenon appeared about the area in the microspheres (Figure 6d), indicating which the terminal carboxyl groups of PA66 had been chemically bonded Using the amino teams around the area from the microspheres through the extrusion response, which wrecked the regularity in the floor of the microspheres (Figure 6b, sleek area and no peeling phenomenon) and led for the Main–shell separation of the microspheres (Figure 6d), confirming the occurrence of the in situ loading reaction.